

The influence of the ZhS6K powder Initial characteristics on the alloy microrelief features after selective laser melting
https://doi.org/10.22349/1994-6716-2022-109-1-101-119
Abstract
The analysis of the ZhS6K alloy granules appearance, their surface and internal structure, as well as the chemical composition by volume and structural elements is carried out. The formation control possibility is shown for desired state of interfaces (tracks, crystallization cells, hatch block boundaries, grains, phases, discontinuities - pores and cracks) through the fractional composition, packing density during filling, scanning speed that provide a more solid and qualitative material state of the sample. The initial state of the samples structure was studied. A connection between the structure of crystallization cells boundaries, dispersed par- ticles and the fragments structure has been established. It is shown that all investigated samples have a differ- ent structure at the same power and scanning strategy. The analysis was carried out by optical metallography and scanning (raster) electron microscopy (SEM) methods.
Keywords
About the Authors
A. N. RaevskikhRussian Federation
17 Radio St, 105005 Moscow
E. B. Chabina
Russian Federation
Cand Sc. (Eng)
17 Radio St, 105005 Moscow
E. V. Filonova
Russian Federation
17 Radio St, 105005 Moscow
References
1. Kablov, E.N., Additivnye tekhnologii – dominanta natsionalnoi tekhnologicheskoi initsiativy [Additive technologies: a dominant of national technology initiative], Intellekt i tekhnologii, 2015, No 2 (11), pp. 52–55.
2. Kablov, E.N., Nastoyashchee i budushchee additivnykh tekhnologii [Additive technologies: present-day and the future], Metally Evrazii, 2017, No 1, pp. 2–6.
3. Kablov, E.N., Klyuchevaya problema – materialy [Key problem – materials], Tendentsii i orientiry innovatsionnogo razvitiya Rossii, Moscow: VIAM, 2015, pp. 458–464.
4. Gu, D.D., Meiners, W., Wissenbach, K., Poprawe, R., Laser additive manufacturing of metallic components: materials, processes and mechanisms, International Materials Reviews, 2012, V. 57, No 3, pp. 133–164.
5. Thornton, A., Saad, J., Clayton, J., Measuring the critical attributes of AM powders, Metal Powder Report, 2019, V. 74, Issue 6, pp. 314–319. DOI: 10.1016/j.mprp.2019.01.006.
6. Kalinina, N.E., Kalinin, V.T., Grekova, M.V., Mamchur, S.I., Nosova, T.V., Mekhanicheskie i korrozionnye svoistva mnogokomponentnykh splavov, modifitsirovannykh dispersnymi kompozitsiyami [Mechanical and corrosion properties of multicomponent alloys modified with dispersed com- positions], Stroitelstvo, materialovedenie, mashinostroenie: Starodubovskie chteniya, 2018, pp. 146–150. DOI: 10.30838/P.CMM.2415. 200418.146.22
7. Chabina, E.B., Filonova, E.V., Raevskikh, A.N., Tsvetkova, E.V., Zavisimost defektnosti struktury zharoprochnogo nikelevogo splava ot tekhnologicheskikh parametrov selektivnogo lazernogo splavleniya [Dependence of the high-temperature nickel alloy’s structure defectiveness on the technological parameters of selective laser melting], Metallovedenie i termicheskaya obrabotka metallov, 2018, No 6 (756), pp. 33–41.
8. Evgenov, A.G., Nerush, S.V., Vasilenko, S.A., Poluchenie i oprobovanie melkodispersnogo metallicheskogo poroshka vysokokhromistogo splava na nikelevoy osnove primenitelno k lazernoy LMD-naplavke [The obtaining and testing of the fine-dispersed metalpowder of the high-chromium nickelbased alloy on LMD-metal deposition], Trudy VIAM, 2014, No 5, p. 4. URL: http://www.viam-works.ru (ref- erence date 15/10/2017). DOI: 10.18577/2307-6046-2014-0-5-4-4
9. Evgenov, A.G., Shcherbakov, S.I., Rogalev, A.M., Oprobovanie poroshkov zharoprochnykh splavov EP718 i EP648 proizvodstva VIAM dlya remonta detaley GTD metodom lazernoy gazopo- roshkovoy naplavki [Application of heat resistant EP718 and EP648 alloys powders to repair of laser gas turbine engine parts by braze], Aviatsionnye materialy i tekhnologii [Aviation Materials and Technologies], 2016, S1, pp. 16–23. DOI 10.18577/2071-9140-2016-0-S1-16-23
10. Lashko, N.F., Zaslavskaya, L.V., Kozlova, M.N. et al., Fiziko-khimichesky fazovy analiz staley i splavov [Physicochemical phase analysis of steels and alloys], Moscow: Metallurgiya, 1978.
11. Betteridge, W., Zharoprochnye splavy tipa nimonik [Heat-Resistant Alloys of the Nimonic type], Moscow, 1961.
12. Thijs, L., Verhaeghe, F., Craeghs, T., Humbeeck, J.V., Kruth, J.P., A study of the microstructural evolution during selective laser melting of Ti-6Al-4V, Acta Materialia, 2010, V. 58, pp. 3303–3312.
13. Prashanth K.G., Scudino S., Maity T., Das J., Eckert J. Is the energy density a reliable parameter for materials synthesis by selective laser melting, Materials Research Letters, 2017, V. 5, No 6, pp. 386–390. DOI: 10.1080/21663831.2017.1299808.
14. Li, R., Liu, J., Shi, Y., Wang, L., Jiang, W., Balling behavior of stainless steel and nickel powder during selective laser melting process, The International Journal of Advanced Manufacturing Technology, 2012, V. 59, pp. 1025–1035.
15. Sukhov, D.I., Mazalov, P.B., Nerush, S.V., Khodirev, N.A., Vliyanie parametrov selektivnogo lazernogo splavleniya na obrazovanie poristosti v sintezirovannom materiale korrozionnostoikoi stali [The influence of SLS parameters on pores formation in stainless steel material], Trudy VIAM, 2017, No 8 (56), p. 4. URL: http://www.viam-works.ru (reference date 11.01.2018). DOI 10.18577/2307-6046-2017-0-8-4-4.
16. Terhaar, J., Poppenhдger, J., Bokelmann, D., Schafstall, H., Kelkar K., Considering the solidification structure of var ingots in the numerical simulation of the cogging process, Superalloys 2010: 7th international symposium on superalloys 718 and derivatives TMS, The minerals, metals and materials society, 2010, pp. 65–77. DOI: 10.7449/2010/Superalloys_2010_65_77.
17. Vernon Cole, J., Northrop, P.W.C., Tan, X.G., Chou, K., Wang, X., Keya T., High-Fidelity Modeling and Materials Characterization of Inconel 718 Component Fabrication by Selective Laser Melting Additive Manufacturing, 2016 JANNAF TIM-Additive Manufacturing, 2016, pp. 1–24. URL: https://ntrs.nasa.gov/api/citations/20160012080/downloads/20160012080.pdf (reference date 07/02/2022).
18. Lapteva, M.A., Belova, N.A., Raevskikh, A.N., Filonova, E.V., Issledovanie zavisimosti sherokhovatosti, morfologii poverkhnosti i kolichestva defektov struktury ot moshchnosti lazera, skorosti skanirovaniya i tipa shtrikhovki v zharoprochnom splave, sintezirovannom metodom SLS [Dependence of roughness, surface morphology structure and number of defects on the power of the laser, scanning speed and the type of hatching in the high-temperature alloys synthesized by SLS], Trudy VIAM, 2016, No 9, p. 9. URL: http://www.viam-works.ru (reference date 17/02/2021). DOI: 10.18577/2307-6046-2016-0-9-9-9.
19. Tsivilsky, I.V., Gilmutdinov, A.H., Hamidullin, B.A., Nikiforov, S.A., Rublya, R.S., Matematicheskoe modelirovanie dinamiki i fazovykh perekhodov v poroshkovykh materialakh v protsesse additivnogo proizvodstva [Mathematical modeling of dynamics and phase transitions in powder materials in additive manufacturing], Proceedings of the 12th All-Russian conference on testing and research of materials properties “TestMat” on the topic “Modern aspects of structural-phase transformations research in the creation of new generation materials”, Moscow: VIAM, 2020, pp. 172–186.
20. Shalin, R.E., Svetlov, I.L., Kachanov, E.B., Toloraya, V.N., Gavrilin, O.S., Monokristally nikelevykh zharoprochnykh splavov [Monocrystals of nickel heat-resistant alloys], Moscow: Mashinostroenie, 1997.
21. Markovich, O.V., Orekhov, N.G., Razumovsky, I.M., Diffuzionnaya pronitsaemost i strukturnoe sostoyanie vnutrennikh poverkhnostey razdela v monokristallakh zharoprochnogo nikelevogo splava [Diffusion permeability and structural state of internal interfaces in heat-resistant nickel alloy’s single crystals], Fizika metallov i metallovedenie, 1994, V. 78, No 2, pp. 1–15. URL: https://viam.ru/sites/default/files/scipub/1993/1993-201486.pdf (reference date 22/03/2021).
22. Evgenov, A.G., Lukina, E.A., Korolyov, V.A., Osobennosti protsessa selektivnogo lazernogo sinteza primenitelno k liteynym splavam na osnove nikelya i intermetallida Ni3Al [Features of process of the selection laser synthesis with reference to cast alloys on the basis of nickel and Ni3Al intermetallic compound], Novosti materialovedeniya. Nauka i tekhnika, 2016, V. 5, No 23, pp. 3–11. URL: http://materialsnews.ru/plugins/content/journal/uploads/articles/pdf/219.pdf (reference date 07/02/2022).
23. Raevskikh, A.N., Chabina, E.B., Filonova, E.V., Belova, N.A., Vozmozhnosti metoda difraktsii obratnootrazhennykh elektronov dlya issledovaniya osobennostey struktury nikelevykh zharoprochnykh splavov, poluchennykh selektivnym lazernym splavleniem [Possibilities of the backscattered electron diffraction (EBSD) method for studying the structural features of nickel heat-resistant alloys obtained by selective laser alloying], Trudy VIAM, 2017, V. 12 (60), p. 12. URL: http://www.viam-works.ru (reference date 10.03.2021). DOI: 10.18577/2307-6046-2017-0-12-12-12.
24. Gockel, J., Beuth, J., Understanding Ti-6Al-4V Microstructure Control in Additive Manufacturing via Process Maps, Proceedings of Solid Freeform Fabrication Symposium, Austin, Texas, 2013, pp. 666–674. URL: http://utw10945.utweb.utexas.edu/Manuscripts/2013/2013-53-Gockel.pdf (reference date 07/02/2022).
25. Kablov, E.N., Innovatsionnye razrabotki VIAM po realizatsii “Strategicheskih napravlenii razvitiya materialov i tekhnologii ikh pererabotki na period do 2030 goda” [VIAM Innovative developments for “Strategic directions for the materials and their processing technologies development for the period up to 2030”], Aviatsionnye materialy i tekhnologii, 2015, No 1, pp. 3–33. DOI 10.18577/2071-9140-2015-0-1-3-33.
Review
For citations:
Raevskikh A.N., Chabina E.B., Filonova E.V. The influence of the ZhS6K powder Initial characteristics on the alloy microrelief features after selective laser melting. Voprosy Materialovedeniya. 2022;(1(109)):101-119. (In Russ.) https://doi.org/10.22349/1994-6716-2022-109-1-101-119