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Study of stress corrosion cracking susceptibility of irradiated ferrite-martensitic stainless steel 07Kh12NMFB in supercritical water. Part 2. Development of corrosion crack identification technique and analysis of autoclave test results

https://doi.org/10.22349/1994-6716-2023-116-4-245-259

Abstract

The studies of stress corrosion cracking have been carried out for the stainless ferritic-martensitic steel with chromium content of 12% irradiated to a damage neutron dose of ~12 dpa. This steel was chosen as a candidate material for the internals of supercritical water-cooled reactors (SWCR).

The first part of the paper was devoted to autoclave testing of specially designed disk specimens under constant load in a supercritical water environment (at 450°C and 250 atm pressure). In this part of the article the developed technique for corrosion cracks identification is presented and analysis of autoclave tests results is performed.

As a result of the experiments performed, the threshold stress values below which stress corrosion cracking initiation doesn’t occur. The values of threshold stresses are determined for the studied steel irradiated at temperatures of 390 and 550°C. Possible mechanisms of stress corrosion cracking of the studied steel are analyzed and directions for further research are proposed.

About the Authors

B. Z. Margolin
NRC «Kurchatov Institute» – CRISM «Prometey»
Russian Federation

Dr Sc (Eng)

49 Shpalernaya St, 191015 St Petersburg



N. E. Pirogova
NRC «Kurchatov Institute» – CRISM «Prometey»
Russian Federation

Cand Sc. (Eng)

49 Shpalernaya St, 191015 St Petersburg



A. A. Sorokin
NRC «Kurchatov Institute» – CRISM «Prometey»
Russian Federation

Cand Sc. (Eng)

49 Shpalernaya St, 191015 St Petersburg



V. I. Kohonov
NRC «Kurchatov Institute» – CRISM «Prometey»
Russian Federation

49 Shpalernaya St, 191015 St Petersburg



A. V. Dub
Private Enterprise for Nuclear Industry Scientific Developement «Science and Innovations»
Russian Federation

Dr Sc (Eng)

44 bld 4 Bolshaya Ordynka St, 119017 Moscow



I. A. Safonov
Private Enterprise for Nuclear Industry Scientific Developement «Science and Innovations»
Russian Federation

Cand Sc. (Eng)

44 bld 4 Bolshaya Ordynka St, 119017 Moscow



References

1. Karzov, G.P., Margolin, B.Z., Shvetsova, V.A., Fiziko-mekhanicheskoe modelirovanie protsessov razrusheniya [Physical and mechanical modeling of destruction processes], St Petersburg: Politekhnika, 1993.

2. Hancock, J.W., Mackenzi, A.C., On the mechanisms of ductile failure in high-strength steels subjected to multi-axial stress state, J. Mech. Phys. Solids., 1976, V. 24 (213), pp. 147–149.

3. Klueh, R.L., Nelson, A.T., Ferritic/martensitic steels for next-generation reactors, J. Nucl. Mater., 2007, V. 371, pp. 37–52.

4. Patra, A., Mc Dowell, D. L., Continuum modeling of localized deformation in irradiated bcc materials, J. Nucl. Mater., 2013, V. 432, pp. 414–427.

5. Zinkle, S.J., Hashimoto, N., Matsukawa, Y., et al., Microstructures of irradiated and mechanically deformed metals and alloys: fundamental aspects, Materials Research Society symposia proceedings “Materials Research Society”,·2004, January.

6. Luppo, M.I., Bailat, C., Schӓublin, R., et al. Tensile properties and microstructure of 590 MeV proton-irradiated pure Fe and a Fe-Cr alloy, J. Nucl. Mater., 2000, V. 283–287, pp. 483–487.

7. Margolin, B., Sorokin, A., Pirogova, N., Analysis of mechanisms inducing corrosion cracking of irradiated austenitic steels and development of a model for prediction of crack initiation, Engineering Failure Analysis, 2020, V. 107.


Review

For citations:


Margolin B.Z., Pirogova N.E., Sorokin A.A., Kohonov V.I., Dub A.V., Safonov I.A. Study of stress corrosion cracking susceptibility of irradiated ferrite-martensitic stainless steel 07Kh12NMFB in supercritical water. Part 2. Development of corrosion crack identification technique and analysis of autoclave test results. Voprosy Materialovedeniya. 2023;(4(116)):245-259. (In Russ.) https://doi.org/10.22349/1994-6716-2023-116-4-245-259

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ISSN 1994-6716 (Print)