METALS SCIENCE. METALLURGY
The temperature-strain conditions of dynamic and static recrystallization during hot deformation were determined at a rate of 1 sec–1 for medium-carbon steel microalloyed with titanium, boron, and vanadium containing different amounts of niobium. It was found that under hot rolling conditions niobium prevents the completion of dynamic recrystallization, and at temperatures below 970°C it drastically slows down static recrystallization in the pauses between successive reductions.
It is known that the solidification of melts under the influence of external factors leads to the formation of a fine-grained structure in the work pieces which improves the mechanical characteristics of finished metal products. The production of lengthy profiles with a high level of mechanical properties in a short production cycle is a complex interdisciplinary task of great practical importance. The paper presents results of research of the properties of products from aluminum alloy V95, which were obtained by continuous vertical casting combined with deformation in the solid-liquid state during solidification. A diagram of a device that implements such a process of combining is presented; its operation is reviewed. Also, a description is given of a method for producing flat work pieces and sample preparation for studying their mechanical characteristics and microstructure.
As research shows the metal products have a fine-grained structure with a dense directional arrangement of dislocations. The grain boundaries are wide, uneven, consisting of grids and dislocation plexuses. During the melt solidification a thin directional dislocation structure is formed in the crystallizer of the device providing increase of the mechanical characteristics of metal products without additional processing, and there are no shrinkage defects. The possibility of obtaining long metal products with high mechanical characteristics for a short production cycle with reduced power costs was shown.
FUNCTIONAL MATERIALS
The paper presents results of studies of the optical and electromagnetic properties of the WO3/rGO electrochromic nanocomposite films obtained by mechanical spraying of a water-based dispersed solution with WO3/GO particles and heat treatment (annealing) at a temperature of 300°C in an inert argon atmosphere for 24 hours. As a result, an electrically conductive phase of reduced graphene oxide rGO and crystalline WO3 were formed.
POLYMERIC COMPOSITE MATERIALS
CORROSION AND PROTECTION OF METALS
The paper studies stress corrosion cracking (SCC) of low carbon low alloyed steels. It is shown that the use of eddy current method allows us to evaluate modifications of fine structures associated with the processes of initiation and growth of stress corrosion cracks. The dependences of the incubation time on the value of the macroelasticity limit σ0 are given. It is noted that the increase in the value of σ0 leads to an increase in the time before the initiation of the first crack. This can be explained: the limit of macroelasticity determines the beginning of microplastic flow in the material. On the basis of experimental data, the analytical dependence of the incubation period of the SCC on the value of the macroelasticity limit is obtained. The calculation error did not exceed 10%. A parameter is proposed for assessing the state of the material subject to SCC. It allows recording the passage of the stages of accumulation of micro-damages and the moment of exhaustion of a significant part of the material resource before the appearance of multiple surface macro-cracks according to the data of eddy current measurements.